Download Advanced practical organic chemistry by Leonard, John; Lygo, B.; Procter, Garry PDF

By Leonard, John; Lygo, B.; Procter, Garry

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Chromatography data HPLC and/or GC are often used to determine purity or isomer ratios present in a mixture. When using these techniques, it is essential to record the conditions, the means of detection, and the type of column used as well as retention times. 11. Other data The preceding listed data are those that are essential for the characterization of most organic molecules. , UV-vis, optical rotatory dispersion, and circular dichroism). Your supervisor should be able to advise on which additional types of data are appropriate.

Even for reactions that do not proceed to give the desired product, it is important to have a good record of the procedure that can be referred to later. For instance, after several attempts to bring about a reaction have failed, it is often possible to learn from what has been done previously to design and carry out a more successful procedure. 3. It should be the main index point that will enable you to find experimental, literature, and spectroscopic data on any compound that you have synthesized.

The advantage of this system is that it is easy to see at a glance whether a particular piece of data has been obtained for a compound. However, two disadvantages of the fixed-format data sheet are as follows: it does not provide the ­flexibility that is often required to record diverse types of data used to characterize any particular compound, and it tends to encourage the mistaken idea that every compound requires the same characterization data. 3. This would need to be generated within a word-processing package so that it can be easily modified.

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