By Harry G. Brittain
Even if the legit compendia outline a drug substance as to id, purity, energy, and caliber, they typically don't offer different actual or chemical information, nor do they record equipment of synthesis or pathways of actual or organic degradation and metabolism. Such info is scattered through the medical literature and the records of pharmaceutical laboratories. Edited by way of the affiliate Director of Analytical study and improvement for the yankee organization of Pharmaceutical Scientists, Analytical Profiles of Drug elements and Excipients brings this data jointly into one resource. The scope of the sequence has lately been multiplied to incorporate profiles of excipient fabrics.
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Extra info for Analytical Profiles of Drug Substances, Excipients, and Related Methodology
The absorbance maximum for this system was determined to be 225 nm. 2 Vibrational Spectroscopy The infra red absorption spectrum of benzoic acid was obtained in a potassium bromide disc (using approximately 2 mg of benzoic acid dispersed in 200 mg KBr), and recorded on a Jasco 5300 FTIR spectrophotometer. The spectrum thusly obtained is shown in Figure 6, and the assignment of the characteristic bands is given in Table 3. 1 Nuclear Magnetic Resonance Spectrometry 'H-NMR Spectrum The 90 MHz 'H-NMR spectrum of benzoic acid shown in Figure 7 was obtained in deuterated chloroform using a Hitachi R- I900 FT-NMR spectrometer.
Reported the determination of deuterated benzoic acid in human urine by using high-field deuterium NMR . The observed magnitudes of the I3C and *H-2,6resonances were used to calculate the quantities of 7-I3Cand 2,6-2Hbenzoic acid present in the samples. The lower limit of this method was approximately 60 nmol/mL. 5. 1 Solid-state Stability Benzoic acid has been found to be stable at normal temperature and pressure conditions, and hazardous polymerization will not occur under normal condition [44-461.
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